Advanced Ceramics Progress

Advanced Ceramics Progress

A Comparative Study of Microstructure and Mechanical Properties in Copper Processed by Simple Shear Extrusion and Elliptical Cross-Section Spiral Equal-Channel Extrusion

Document Type : Original Research Article

Author
Instructor, Department of Mechanical Engineering, Hakim Sabzevari University, Sabzevar, Iran.
Abstract
One of the well-known approaches for producing ultrafine-grained and nanostructured materials is severe plastic deformation (SPD), which has attracted significant attention in recent years. This study investigates the microstructural evolution and mechanical properties of commercially pure copper processed by two SPD methods: Simple Shear Extrusion (SSE) and Spiral Equal-Channel Extrusion with an Elliptical Cross-Section (ECSEE). Samples underwent four sequential extrusion passes at room temperature using both techniques and were subsequently characterized through metallography, microhardness measurements, tensile testing, and forming force analysis. The results demonstrate a substantial enhancement in mechanical properties and grain refinement with each additional pass for both processes. However, the ECSEE method, which imposes more severe plastic strain, yielded superior results. Specifically, after four passes, the ECSEE-processed samples achieved an ultimate tensile strength of 349 MPa and a microhardness of 166 HV, representing increases of 104% and 9%, respectively, compared to the annealed condition. In contrast, the SSE method, which applies lower and more gradual strain, resulted in an ultimate tensile strength of 242 MPa and a microhardness of 139 HV after four passes. Microstructural analysis revealed reductions in grain size of 28% and 17% for the ECSEE- and SSE-processed samples, respectively, after the fourth pass. Furthermore, the SSE method required a lower forming force due to the lower strain imposed. The findings conclusively indicate that the ECSEE process produces superior microstructural characteristics and enhanced mechanical behavior, including strength, microhardness, and ductility, compared to the SSE method.
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Subjects

1.      Abenojar, J., Velasco, F., & Martínez, M. A. (2008). Optimization of processing parameters for the Al–10% B4C system obtained by mechanical alloying. Journal of Materials Processing Technology, 328(1–2), 222–229. 10.1016/j.jmatprotec.2006.11.122
2.      Bagherpour, E., Pardis, N., Reihanian, M., & Ebrahimi, R. (2016). Microstructure quantification of ultrafine-grained pure copper fabricated by simple shear extrusion (SSE) technique. Materials Science and Engineering: A, 674, 221–231. https://doi.org/10.1016/j.msea.2016.08.001
3.      Balali, M., Beynaghi, M., & Khosravi, M. (2021). Investigation of simple shear extrusion steel mold and mechanical properties of nanostructured extruded samples of Al6061. International Journal of Iron and Steel Society of Iran, 18(1), 106–112. 10.22034/ijissi.2021.540568.1211
4.      Balali, M., Limouei, M. B., & Balali, M. (2018). Study on optimization of parameters affecting simple shear extrusion of pure copper to fabricate fine-grain structure. Transactions of the Indian Institute of Metals, 71(3), 605–616. https://doi.org/10.1007/s12666-017-1193-8
5.      Balali,M , Seyedkashi,S M H , Hasanabadi,A , Gorji,H , Baseri,H and Khosravi,M . (2025). A New Ultrasonic-assisted Simple Shear Extrusion Process in Production of Ultrafine Grained Copper. International Journal of Engineering, 38(4), 908-920.  10.5829/ije.2025.38.04a.19
6.      Courtney, T. H. (2000). Mechanical behavior of materials (2nd ed., pp. 85–87). Waveland Press.
7.      El-Danaf, E. A. (2008). Mechanical properties and microstructure evolution of 1050 aluminum severely deformed by ECAP to 16 passes. Materials Science and Engineering: A, 487(1–2), 189–200. https://doi.org/10.1016/j.msea.2007.10.013
8.      El-Danaf, E. A., Soliman, M. S., Almajid, A. A., & El-Rayes, M. M. (2007). Enhancement of mechanical properties and grain size refinement of commercial purity aluminum 1050 processed by ECAP. Materials Science and Engineering: A, 458(1–2), 226–234. https://doi.org/10.1016/j.msea.2006.12.077
9.      Faraji, G., Kim, H. S., & Torabzadeh Kashi, H. (2018). Severe plastic deformation: Methods, processing and properties. Elsevier. 0128135670, 9780128135679
10.    Ge, Z., et al. (2024). Effect of Zn addition combined with a novel screw twist extrusion technology on the microstructure, texture as well as the ductility of Mg-xZn-1Mn alloys. Journal of Alloys and Compounds, 984, 173995. https://doi.org/10.1016/j.jallcom.2024.173995
11.    Gubicza, J., Chinh, N. Q., Krállics, G., Schiller, I., & Ungár, T. (2006). Microstructure of ultrafine-grained FCC metals produced by severe plastic deformation. Current Applied Physics, 6(2), 194–199. https://doi.org/10.1016/j.cap.2005.07.039
12.    Haasen, P. (1996). Physical metallurgy. Cambridge university press.
13.    Hall, E. O. (1951). The deformation and ageing of mild steel: III. Discussion of results. Proceedings of the Physical Society Section B, 64(9), 747–753. 10.1088/0370-1301/64/9/303
14.    Hosseini, S. A., & Manesh, H. D. (2009). High-strength, high-conductivity ultra-fine grain commercial pure copper produced by the ARB process. Materials & Design, 30(8), 2911–2918. https://doi.org/10.1016/j.matdes.2009.01.012
15.    Janeček, M., Čížek, J., Gubicza, J., & Vrátná, J. (2012). Microstructure and dislocation density evolutions in MgAlZn alloy processed by severe plastic deformation. Journal of Materials Science, 47(22), 7860–7869. https://doi.org/10.1007/s10853-012-6538-4
16.    Latypov, M. I., Beygelzimer, Y., & Kim, H. S. (2013). Comparative analysis of two twist-based SPD processes: Elliptical cross-section spiral equal-channel extrusion vs. twist extrusion. Materials Transactions, 54(9), 1587–1591. https://doi.org/10.2320/matertrans.MH201315
17.    Li, J., Wang, C., Li, F., & Liu, J. (2021). Microstructure and mechanical properties of pure Mg after spiral equal-channel extrusion. Materials Science and Technology, 37(4), 384–394. https://doi.org/10.1080/02670836.2021.1901366
18.    Mills, K., Li, H., Luzin, V., & Kent, D. (2025). Influence of ECAP deformation routes on grain refinement, mechanical properties and texture of zinc. Materials Science and Engineering: A, 149066. https://doi.org/10.1016/j.msea.2025.149066
19.    Pardis, N., & Ebrahimi, R. (2009). Deformation behavior in simple shear extrusion (SSE) as a new severe plastic deformation technique. Materials Science and Engineering: A, 527(1–2), 355–360. https://doi.org/10.1016/j.msea.2009.08.051
20.    Salishchev, G. A., Zaripova, R. G., Galeev, R. M., & Valiakhmetov, R. (1995). Nanocrystalline structure formation during severe plastic deformation in metals and their deformation behavior. Nanostructured Materials, 6(5–8), 913–916. https://doi.org/10.1016/0965-9773(95)00208-1
21.    Sevillano, J. G., Van Houtte, P., & Aernoudt, E. (1980). Large strain work hardening and textures. Progress in materials science, 25(2-4), 69-134.  https://doi.org/10.1016/0079-6425(80)90001-8
22.    Tork, N. B., Pardis, N., & Ebrahimi, R. (2013). Investigation on the feasibility of room temperature plastic deformation of pure magnesium by simple shear extrusion process. Materials Science and Engineering: A, 560, 34–39. https://doi.org/10.1016/j.msea.2012.08.085
23.    Tsuji, N., Ito, Y., Saito, Y., & Minamino, Y. (2002). Strength and ductility of ultrafine-grained aluminum and iron produced by ARB and annealing. Scripta Materialia, 47(12), 893–899. 10.1016/S1359-6462(02)00282-8
24.    Valiev, R. Z. (Ed.). (1996). Ultra-fine-grained materials prepared by severe plastic deformation. Annales de Chimie Science des Matériaux, 21, 369.
25.    Valiev, R. Z., Alexandrov, I. V., & Islamgaliev, R. K. (1998). Nanocrystalline materials: Science and technology. In G. M. Chow & N. I. Noskova (Eds.), NATO ASI Series (p. 121). Kluwer Academic Publishers.
26.    Valiev, R. Z., Islamgaliev, R. K., & Alexandrov, I. V. (2000). Bulk nanostructured materials from severe plastic deformation. Progress in Materials Science, 45(2), 103–189. https://doi.org/10.1016/S0079-6425(99)00007-9
27.    Valiev, R. Z., Korznikov, A. V., & Mulyukov, R. R. (1993). Structure and properties of ultrafine-grained materials produced by severe plastic deformation. Materials Science and Engineering: A, 168(2), 141–148. https://doi.org/10.1016/0921-5093(93)90717-S
28.    Valiev, R. Z., & Langdon, T. G. (2006). Principles of equal-channel angular pressing as a processing tool for grain refinement. Progress in Materials Science, 51(7), 881–981. https://doi.org/10.1016/j.pmatsci.2006.02.003
29.    Wang, C., Li, F., Liu, J., & Li, J. (2013). Deformation analysis of elliptical cross-section spiral equal channel extrusion technique. Rare Metal Materials and Engineering, 42(4), 679–683. https://doi.org/10.1016/S1875-5372(13)60055-7
30.    Wang, C., Li, F., & Liu, J. (2018). Deformational features and microstructure evolution of copper fabricated by a single pass of the elliptical cross-section spiral equal-channel extrusion (ECSEE) process. Journal of Materials Engineering and Performance, 27(6), 2967–2977. https://doi.org/10.1007/s11665-018-3265-2
31.    Zhou, T., et al. (2024). Excellent strength-ductility synergy properties of Mg–Sn–Zn–Zr alloy mediated by a novel differential thermal ECAP (DT-ECAP). Materials Science and Engineering: A, 899, 146469. https://doi.org/10.1016/j.msea.2024.146469
Volume 11, Issue 4
Autumn 2025
Pages 21-30

  • Receive Date 08 June 2026
  • Revise Date 17 June 2026
  • Accept Date 05 July 2026