Advanced Ceramics Progress

Advanced Ceramics Progress

Heat Treatment of Pulsed Electroplated Nickel Deposited on AA2024 Aluminum

Document Type : Original Research Article

Authors
A. Khiabani 1
Z. S. Seyedraoufi 1
M. Heydarzadeh Sohi 2
1 Department of Metallurgy and Materials Engineering, Karaj Branch, Islamic Azad University, Karaj, Alborz, Iran
2 School of Metallurgy and Materials, College of Engineering, University of Tehran, Tehran, Tehran, Iran
10.30501/acp.2021.252211.1048
Abstract
In this study, pure nickel was deposited on AA2024 aluminum via pulsed electrodeposition using two duty cycles (25 % and 50 %) at two different frequencies (50 and 100 Hz). The coated specimens were then heat-treated in an argon atmosphere at 500 °C for one hour. The treated specimens were characterized using Optical Microscope (OM), Scanning Electron Microscope (SEM) equipped with energy dispersive spectrometer (EDS), and X-Ray Diffraction (XRD) analysis. According to the results, the coatings were thickened upon increasing the duty cycle and frequency. Heat treatment of the nickel-coated specimen under the duty cycle of 25 % and frequency of 50 Hz experienced formation of Al3Ni intermetallic compound at the interface of the nickel coating and aluminum-based substrate. Heat treatment adversely affected the corrosion resistance of the nickel-coated specimens. Nevertheless, the specimens with Al3Ni intermetallic compound at their interface demonstrated better corrosion resistance among heat-treated materials.
Keywords
AA2024 aluminum
Pulse Electroplating
Heat Treatment
Al3Ni Intermetallic Compound
Corrosion

Subjects

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  • Receive Date 14 May 2021
  • Revise Date 16 June 2021
  • Accept Date 29 June 2021